Toward a better description of gallo-phosphate materials in solid-state NMR 1D and 2D correlation studies

Toward a better description of gallo-phosphate materials in solid-state NMR : 1D and 2D correlation studies

Copyright 2006 John Wiley & Sons, Ltd.

Bibliographische Detailangaben
Veröffentlicht in:Magnetic resonance in chemistry : MRC. - 1985. - 44(2006), 8 vom: 05. Aug., Seite 770-5
1. Verfasser: Montouillout, Valérie (VerfasserIn)
Weitere Verfasser: Morais, Cláudia M, Douy, André, Fayon, Franck, Massiot, Dominique
Format: Aufsatz
Sprache:English
Veröffentlicht: 2006
Zugriff auf das übergeordnete Werk:Magnetic resonance in chemistry : MRC
Schlagworte:Journal Article
Beschreibung
Zusammenfassung:Copyright 2006 John Wiley & Sons, Ltd.
We show that weak 2J(71Ga-O-31P), typically approximately 12 Hz in GaPO4, can be used to efficiently establish heteronuclear 31P-71Ga correlation using a MAS HMQC experiment in gallo-phosphate materials. The experiment demonstrated for cristobalite GaPO4 is then applied to Ga(PO3)3, where it allows the differentiation of the signature of three different Ga sites overlapping in the 1D spectrum
Beschreibung:Date Completed 29.08.2007
Date Revised 23.08.2006
published: Print
Citation Status PubMed-not-MEDLINE
ISSN:0749-1581