Time-Resolved Simultaneous SAXS/WAXS of the Drawing of Polyethylene at the Daresbury SRS

A system has been developed which represents a significant advance in the quality and extent of small- and wide-angle X-ray scattering data (SAXS and WAXS) that can be recorded simultaneously with strain data during the drawing and annealing of polymer materials. WAXS data are recorded using a Photo...

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Veröffentlicht in:Journal of synchrotron radiation. - 1994. - 3(1996), Pt 2 vom: 01. März, Seite 84-90
1. Verfasser: Hughes, D J (VerfasserIn)
Weitere Verfasser: Mahendrasingam, A, Heeley, E L, Oatway, W B, Martin, C, Towns-Andrews, E, Fuller, W
Format: Aufsatz
Sprache:English
Veröffentlicht: 1996
Zugriff auf das übergeordnete Werk:Journal of synchrotron radiation
Schlagworte:Journal Article
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245 1 0 |a Time-Resolved Simultaneous SAXS/WAXS of the Drawing of Polyethylene at the Daresbury SRS 
264 1 |c 1996 
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520 |a A system has been developed which represents a significant advance in the quality and extent of small- and wide-angle X-ray scattering data (SAXS and WAXS) that can be recorded simultaneously with strain data during the drawing and annealing of polymer materials. WAXS data are recorded using a Photonic Science charge-coupled-device area detector and SAXS data using a gas-filled multiwire area detector. Strain data, for the region of the specimen from which the SAXS/WAXS data are collected, are calculated from an accurately synchronized continuously recorded video image of the specimen. The system allows X-ray and video image data to be collected as a series of frames with essentially no ;dead-time' between frames. The data are fully two-dimensional and can be collected for a wide range of d spacings. The use of this system to investigate the stress-induced orientation and phase changes during the drawing of a range of grades of commercially available polyethylene is described 
650 4 |a Journal Article 
700 1 |a Mahendrasingam, A  |e verfasserin  |4 aut 
700 1 |a Heeley, E L  |e verfasserin  |4 aut 
700 1 |a Oatway, W B  |e verfasserin  |4 aut 
700 1 |a Martin, C  |e verfasserin  |4 aut 
700 1 |a Towns-Andrews, E  |e verfasserin  |4 aut 
700 1 |a Fuller, W  |e verfasserin  |4 aut 
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