The use of a scanning X-ray microprobe for simultaneous XRF/XRD studies of fly-ash particles

With the opening of the first real ;third-generation' synchrotron source in Grenoble, in fall 1994, X-ray sources of unprecedented brilliances and qualities became available to the scientific community. Different X-ray analytical techniques could now be applied on a level that was unimaginable...

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Veröffentlicht in:Journal of synchrotron radiation. - 1994. - 4(1997), Pt 4 vom: 01. Juli, Seite 228-35
1. Verfasser: Rindby, A (VerfasserIn)
Weitere Verfasser: Engström, P, Janssens, K
Format: Aufsatz
Sprache:English
Veröffentlicht: 1997
Zugriff auf das übergeordnete Werk:Journal of synchrotron radiation
Schlagworte:Journal Article
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245 1 4 |a The use of a scanning X-ray microprobe for simultaneous XRF/XRD studies of fly-ash particles 
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520 |a With the opening of the first real ;third-generation' synchrotron source in Grenoble, in fall 1994, X-ray sources of unprecedented brilliances and qualities became available to the scientific community. Different X-ray analytical techniques could now be applied on a level that was unimaginable only a decade ago. Here are some preliminary results from an experiment where different analytical techniques have been applied on a micrometer level carried out at the most powerful synchrotron microbeam currently available in the world, the microfocus beamline (BL1) at ESRF. This beamline can now provide micrometer-sized X-ray beams with a flux density up to 10(10) photons microm(-2) at an energy of 13 keV and with a bandwidth of 10(-4). In this experiment, X-ray diffraction and X-ray fluorescence have been combined in order to obtain a precise and comprehensive micro-analytical description of micrometer-sized fly ash particles. These types of particles are heavily inhomogeneous with a very irregular shape that makes them inaccessible to conventional micro-analysis. The experiment was performed in a scanning mode and two-dimensional images of different analytical information were reconstructed from the data recorded during the scan. The major features and limitations of this micro-analytical technique will be outlined and different examples on how the analytical information can be used for generating two-dimensional images of the sample will be demonstrated and discussed 
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700 1 |a Janssens, K  |e verfasserin  |4 aut 
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