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231223s2005 xx ||||| 00| ||eng c |
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|a pubmed24n0525.xml
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|a (DE-627)NLM157595978
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|a (NLM)16142840
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|a DE-627
|b ger
|c DE-627
|e rakwb
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|a eng
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| 100 |
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|a Sobarzo-Sánchez, Eduardo
|e verfasserin
|4 aut
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|a Synthesis and total assignment of 1H and 13C NMR spectra of new oxoisoaporphines by long-range heteronuclear correlations
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|c 2005
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|a Text
|b txt
|2 rdacontent
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|a ohne Hilfsmittel zu benutzen
|b n
|2 rdamedia
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|a Band
|b nc
|2 rdacarrier
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| 500 |
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|a Date Completed 28.02.2006
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|a Date Revised 15.11.2006
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|a published: Print
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|a Citation Status MEDLINE
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|a Copyright (c) 2005 John Wiley & Sons, Ltd.
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|a The new oxoisoaporphines 7H-dibenzo[de,h]quinolin-7-one, 5-methoxy-7H-dibenzo[de,h]quinolin-7-one, 5-methoxy-6-hydroxy-7H-dibenzo[de,h]quinolin-7-one, 5-hydroxy-7H-dibenzo[de,h]quinolin-7-one and 5-methoxy-6H-dibenzo[de,h]quinolin-6-one were prepared either by oxidation of their 2,3-dihydro derivatives or by heating (2'-(3,4-dihydro-6,7-dimethoxyisoquinolin-1'-yl)phenyl)methylbenzoate with an acetic acid/sulfuric acid mixture at 100 degrees C. The structures were confirmed and 1H and 13C NMR spectra were completely assigned using two-dimensional NMR techniques
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|a Journal Article
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| 650 |
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|a Research Support, Non-U.S. Gov't
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| 650 |
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|a Aporphines
|2 NLM
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| 650 |
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|a Carbon Isotopes
|2 NLM
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| 650 |
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|a Protons
|2 NLM
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| 700 |
1 |
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|a De la Fuente, Julio
|e verfasserin
|4 aut
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| 700 |
1 |
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|a Castedo, Luis
|e verfasserin
|4 aut
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| 773 |
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|i Enthalten in
|t Magnetic resonance in chemistry : MRC
|d 1985
|g 43(2005), 12 vom: 19. Dez., Seite 1080-3
|w (DE-627)NLM098179667
|x 1097-458X
|7 nnns
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| 773 |
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|g volume:43
|g year:2005
|g number:12
|g day:19
|g month:12
|g pages:1080-3
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|a GBV_USEFLAG_A
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|a SYSFLAG_A
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|a GBV_ILN_350
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|a AR
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|d 43
|j 2005
|e 12
|b 19
|c 12
|h 1080-3
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