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231223s2005 xx ||||| 00| ||eng c |
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|a (DE-627)NLM156872382
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|a (NLM)16052606
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|a DE-627
|b ger
|c DE-627
|e rakwb
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|a eng
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1 |
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|a Kupce, Eriks
|e verfasserin
|4 aut
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1 |
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|a Resolving overlap in two-dimensional NMR spectra
|b nuclear Overhauser effects in a polysaccharide
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|c 2005
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|a Text
|b txt
|2 rdacontent
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|a ohne Hilfsmittel zu benutzen
|b n
|2 rdamedia
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|a Band
|b nc
|2 rdacarrier
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|a Date Completed 05.12.2005
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|a Date Revised 30.08.2005
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|a published: Print
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|a Citation Status MEDLINE
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|a Copyright (c) 2005 John Wiley & Sons, Ltd.
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|a Overlapping resonances in the two-dimensional nuclear Overhauser (NOESY) spectrum of the O-antigenic polysaccharide from Escherichia coli O147 have been resolved by recording a tilted projection of a three-dimensional NOESY-HSQC spectrum, where the carbon-13 and proton evolutions are linked together. Through the introduction of small contributions from the appropriate carbon-13 shifts, a cluster of five unresolved proton peaks is separated into its components without the need to perform the full three-dimensional measurement, a time saving of at least an order of magnitude
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|a Journal Article
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|a Carbon Isotopes
|2 NLM
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|a O Antigens
|2 NLM
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| 650 |
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|a Protons
|2 NLM
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| 700 |
1 |
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|a Nishida, Toshiaki
|e verfasserin
|4 aut
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| 700 |
1 |
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|a Widmalm, Göran
|e verfasserin
|4 aut
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| 700 |
1 |
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|a Freeman, Ray
|e verfasserin
|4 aut
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| 773 |
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|i Enthalten in
|t Magnetic resonance in chemistry : MRC
|d 1985
|g 43(2005), 10 vom: 12. Okt., Seite 791-4
|w (DE-627)NLM098179667
|x 1097-458X
|7 nnns
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| 773 |
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|g volume:43
|g year:2005
|g number:10
|g day:12
|g month:10
|g pages:791-4
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|a GBV_ILN_350
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|a AR
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|d 43
|j 2005
|e 10
|b 12
|c 10
|h 791-4
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