|
|
|
|
| LEADER |
01000naa a22002652 4500 |
| 001 |
NLM156768151 |
| 003 |
DE-627 |
| 005 |
20231223074829.0 |
| 007 |
tu |
| 008 |
231223s2005 xx ||||| 00| ||eng c |
| 028 |
5 |
2 |
|a pubmed24n0523.xml
|
| 035 |
|
|
|a (DE-627)NLM156768151
|
| 035 |
|
|
|a (NLM)16041773
|
| 040 |
|
|
|a DE-627
|b ger
|c DE-627
|e rakwb
|
| 041 |
|
|
|a eng
|
| 100 |
1 |
|
|a Schraml, Jan
|e verfasserin
|4 aut
|
| 245 |
1 |
0 |
|a Characterization of polyphenols from plant materials through their silylation and 29Si NMR spectroscopy-line assignment through 29Si, 13C spin-spin couplings
|
| 264 |
|
1 |
|c 2005
|
| 336 |
|
|
|a Text
|b txt
|2 rdacontent
|
| 337 |
|
|
|a ohne Hilfsmittel zu benutzen
|b n
|2 rdamedia
|
| 338 |
|
|
|a Band
|b nc
|2 rdacarrier
|
| 500 |
|
|
|a Date Completed 05.12.2005
|
| 500 |
|
|
|a Date Revised 21.11.2013
|
| 500 |
|
|
|a published: Print
|
| 500 |
|
|
|a Citation Status MEDLINE
|
| 520 |
|
|
|a Copyright (c) 2005 John Wiley & Sons, Ltd.
|
| 520 |
|
|
|a The lines in (29)Si NMR spectra of silylated polyphenols and some other compounds are difficult to assign owing to the absence of couplings with protons outside the silyl group. The assignment can be derived through small (n)J((29)Si, (13)C) couplings (n > 1). Using a previously described method for measurements of these couplings, the assignment procedure is demonstrated here on three examples of trimethylsilylated phenols: 7-hydroxyflavone, ferulic acid, and quercetin. In some cases the procedure can be used to identify carbon atoms to which the siloxy groups are attached
|
| 650 |
|
4 |
|a Journal Article
|
| 650 |
|
4 |
|a Research Support, Non-U.S. Gov't
|
| 650 |
|
7 |
|a Carbon Isotopes
|2 NLM
|
| 650 |
|
7 |
|a Flavonoids
|2 NLM
|
| 650 |
|
7 |
|a Isotopes
|2 NLM
|
| 650 |
|
7 |
|a Phenols
|2 NLM
|
| 650 |
|
7 |
|a Polyphenols
|2 NLM
|
| 650 |
|
7 |
|a Silicon
|2 NLM
|
| 650 |
|
7 |
|a Z4152N8IUI
|2 NLM
|
| 700 |
1 |
|
|a Blechta, Vratislav
|e verfasserin
|4 aut
|
| 700 |
1 |
|
|a Sýkora, Jan
|e verfasserin
|4 aut
|
| 700 |
1 |
|
|a Soukupová, Ludmila
|e verfasserin
|4 aut
|
| 700 |
1 |
|
|a Curínová, Petra
|e verfasserin
|4 aut
|
| 700 |
1 |
|
|a Pronek, David
|e verfasserin
|4 aut
|
| 700 |
1 |
|
|a Lachman, Jaromír
|e verfasserin
|4 aut
|
| 773 |
0 |
8 |
|i Enthalten in
|t Magnetic resonance in chemistry : MRC
|d 1985
|g 43(2005), 10 vom: 15. Okt., Seite 829-34
|w (DE-627)NLM098179667
|x 1097-458X
|7 nnns
|
| 773 |
1 |
8 |
|g volume:43
|g year:2005
|g number:10
|g day:15
|g month:10
|g pages:829-34
|
| 912 |
|
|
|a GBV_USEFLAG_A
|
| 912 |
|
|
|a SYSFLAG_A
|
| 912 |
|
|
|a GBV_NLM
|
| 912 |
|
|
|a GBV_ILN_350
|
| 951 |
|
|
|a AR
|
| 952 |
|
|
|d 43
|j 2005
|e 10
|b 15
|c 10
|h 829-34
|