Complete assignments of the 1H and 13C resonances of 40-epi-(N1-tetrazolyl)-rapamycin and revised 13C assignments for rapamycin
Copyright 2004 John Wiley & Sons, Ltd.
Veröffentlicht in: | Magnetic resonance in chemistry : MRC. - 1985. - 43(2005), 2 vom: 22. Feb., Seite 174-5 |
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1. Verfasser: | |
Format: | Aufsatz |
Sprache: | English |
Veröffentlicht: |
2005
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Zugriff auf das übergeordnete Werk: | Magnetic resonance in chemistry : MRC |
Schlagworte: | Journal Article Carbon Isotopes Tetrazoles Sirolimus W36ZG6FT64 |
Zusammenfassung: | Copyright 2004 John Wiley & Sons, Ltd. Complete 1H and 13C assignments of 40-epi-(N1-tetrazolyl)-rapamycin (ABT-578) in DMSO-d6 were made using 1H, 13C, DQCOSY, ROESY, TOCSY, HSQC and HMBC spectra. Comparing the assignments with those of rapamycin showed that in the published 13C assignments of rapamycin in DMSO-d6 the shifts for C-12 and C-42 have been interchanged, as well as the shifts for C-1 and C-8 |
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Beschreibung: | Date Completed 30.03.2005 Date Revised 21.11.2013 published: Print Citation Status MEDLINE |
ISSN: | 0749-1581 |