Complete assignments of the 1H and 13C resonances of 40-epi-(N1-tetrazolyl)-rapamycin and revised 13C assignments for rapamycin

Copyright 2004 John Wiley & Sons, Ltd.

Bibliographische Detailangaben
Veröffentlicht in:Magnetic resonance in chemistry : MRC. - 1985. - 43(2005), 2 vom: 22. Feb., Seite 174-5
1. Verfasser: Pagano, Thomas G (VerfasserIn)
Format: Aufsatz
Sprache:English
Veröffentlicht: 2005
Zugriff auf das übergeordnete Werk:Magnetic resonance in chemistry : MRC
Schlagworte:Journal Article Carbon Isotopes Tetrazoles Sirolimus W36ZG6FT64
Beschreibung
Zusammenfassung:Copyright 2004 John Wiley & Sons, Ltd.
Complete 1H and 13C assignments of 40-epi-(N1-tetrazolyl)-rapamycin (ABT-578) in DMSO-d6 were made using 1H, 13C, DQCOSY, ROESY, TOCSY, HSQC and HMBC spectra. Comparing the assignments with those of rapamycin showed that in the published 13C assignments of rapamycin in DMSO-d6 the shifts for C-12 and C-42 have been interchanged, as well as the shifts for C-1 and C-8
Beschreibung:Date Completed 30.03.2005
Date Revised 21.11.2013
published: Print
Citation Status MEDLINE
ISSN:0749-1581