Supported particle track etched polyimide membranes : a grazing incidence small-angle X-ray scattering study

Particle track etched polyimide membranes on silicon substrates covered with a native oxide layer are investigated. Preparation steps similar to the common classical particle track etched membrane production, giving rise to free-standing membranes, are successfully applied to the supported membranes...

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Bibliographische Detailangaben
Veröffentlicht in:Langmuir : the ACS journal of surfaces and colloids. - 1992. - 20(2004), 23 vom: 09. Nov., Seite 10303-10
1. Verfasser: Hermsdorf, N (VerfasserIn)
Weitere Verfasser: Sahre, K, Volodin, P, Stamm, M, Eichhorn, K J, Cunis, S, Gehrke, R, Panagiotou, P, Titz, T, Müller-Buschbaum, P
Format: Aufsatz
Sprache:English
Veröffentlicht: 2004
Zugriff auf das übergeordnete Werk:Langmuir : the ACS journal of surfaces and colloids
Schlagworte:Journal Article
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520 |a Particle track etched polyimide membranes on silicon substrates covered with a native oxide layer are investigated. Preparation steps similar to the common classical particle track etched membrane production, giving rise to free-standing membranes, are successfully applied to the supported membranes. Polyimide films are used as a starting material for a template preparation based on high energy ion irradiation. The film/membrane structure is probed at different length scales by grazing incidence small-angle X-ray scattering at each individual preparation step. In addition, characterization with atomic force microscopy, variable-angle spectroscopic ellipsometry, Fourier transform infrared transmission, and attenuated total reflection spectroscopy is performed. An amount of 6 +/- 1 vol % pores inside the polyimide film is detected. The pores are oriented perpendicular to the substrate surface and have a conical shape, yielding a slightly reduced pore size at the substrate/film interface 
650 4 |a Journal Article 
700 1 |a Sahre, K  |e verfasserin  |4 aut 
700 1 |a Volodin, P  |e verfasserin  |4 aut 
700 1 |a Stamm, M  |e verfasserin  |4 aut 
700 1 |a Eichhorn, K J  |e verfasserin  |4 aut 
700 1 |a Cunis, S  |e verfasserin  |4 aut 
700 1 |a Gehrke, R  |e verfasserin  |4 aut 
700 1 |a Panagiotou, P  |e verfasserin  |4 aut 
700 1 |a Titz, T  |e verfasserin  |4 aut 
700 1 |a Müller-Buschbaum, P  |e verfasserin  |4 aut 
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