Sample-angle feedback for diffraction anomalous fine-structure spectroscopy

Diffraction anomalous fine-structure (DAFS) experiments measure Bragg peak intensities as continuous functions of photon energy near a core-level excitation. Measuring the integrated intensity at each energy makes the experiments prohibitively slow; however, in many cases DAFS can be collected quick...

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Détails bibliographiques
Publié dans:Journal of synchrotron radiation. - 1994. - 5(1998), Pt 3 vom: 01. Mai, Seite 911-3
Auteur principal: Cross, J O (Auteur)
Autres auteurs: Elam, W T, Harris, V G, Kirkland, J P, Bouldin, C E, Sorensen, L B
Format: Article
Langue:English
Publié: 1998
Accès à la collection:Journal of synchrotron radiation
Sujets:Journal Article
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520 |a Diffraction anomalous fine-structure (DAFS) experiments measure Bragg peak intensities as continuous functions of photon energy near a core-level excitation. Measuring the integrated intensity at each energy makes the experiments prohibitively slow; however, in many cases DAFS can be collected quickly by measuring only the peak intensity at the center of the rocking curve. A piezoelectric-actuator-driven stage has been designed and tested as part of a sample-angle feedback circuit for locking onto the maximum of the rocking curve while the energy is scanned. Although software peak-tracking requires only a simple calculation of diffractometer angles, it is found that the additional hardware feedback dramatically improves the reproducibility of the data 
650 4 |a Journal Article 
700 1 |a Elam, W T  |e verfasserin  |4 aut 
700 1 |a Harris, V G  |e verfasserin  |4 aut 
700 1 |a Kirkland, J P  |e verfasserin  |4 aut 
700 1 |a Bouldin, C E  |e verfasserin  |4 aut 
700 1 |a Sorensen, L B  |e verfasserin  |4 aut 
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