An X-ray diffractometer for accurate structural invariant phase determination

Instrumental advances and experimental procedures for determining invariant triplet phases by three-beam X-ray diffraction are presented. A simple X-ray diffractometer is described. It allows the exploitation of the natural linear polarization of synchrotron radiation for eliminating systematic erro...

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Veröffentlicht in:Journal of synchrotron radiation. - 1994. - 10(2003), Pt 3 vom: 01. Mai, Seite 236-41
1. Verfasser: Morelhão, Sérgio L (VerfasserIn)
Format: Aufsatz
Sprache:English
Veröffentlicht: 2003
Zugriff auf das übergeordnete Werk:Journal of synchrotron radiation
Schlagworte:Journal Article
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520 |a Instrumental advances and experimental procedures for determining invariant triplet phases by three-beam X-ray diffraction are presented. A simple X-ray diffractometer is described. It allows the exploitation of the natural linear polarization of synchrotron radiation for eliminating systematic errors in triplet-phase determination. Examples of data-collection procedures with the diffractometer for composing a polarization-dependent set of azimuthal scans are given as well as the suggestion of an analytical procedure for extracting accurate triplet phases 
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